Abstract. A detailed study of AISI and stainless steels (SSs) has been conducted to correlate the degree of sensitization (DOS) measured by the. ASTM A is the specification which governs five practices used to determine if the Practice E—Copper–Copper Sulfate–Sulfuric Acid Test for Detecting. Copper – Copper Sulfate – 16% sulfuric acid, ASTM A – Practice E (Strauss Test) This procedure is conducted to determine the susceptibility of austenitic.

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ASTM A testing is a popular method of choice due to the variety of practices available and the relatively short turnaround for results.

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Wilson Hardness Conversion Chart. For example, many low-carbon and stabilized stainless steels e. The weight loss is calculated after each step, and reveals if the sample has been properly heat-treated.

The test is generally performed for acceptance of materials, but not sufficient for rejection of materials. The test evaluates the resistance of extra-low-carbon steels to sensitization a226 intergranular attack from welding or heat treatment processes.

The ASTM A tests can determine if the proper heat treatment astm a262 practice e performed or if the alloys are in danger of intergranular corrosion occurring in use.

ASTM A Testing: An Overview of Intergranular Corrosion | Element

The Oxalic Astm a262 practice e test is only used to ensure that no corrosion asmt samples are labeled either “Acceptable” or “Suspect”.

Intergranular simply means that the corrosion is taking place between the grains or crystals, which is where sigma phase or chromium carbides are going to form which makes the material susceptible to IGA. These tests are often astm a262 practice e as a qualification test to ensure each batch of stainless steel is properly prepared.

In everyday applications, corrosion varies by materials and solutions. How do you astm a262 practice e the right ASTM corrosion testing method for your material? If materials with incorrect heat treatment enter service, they are liable to crack or fail by intergranular corrosion IGC much more rapidly than properly treated materials; ASTM A is a screening test to help find batches that are incorrectly processed.

We provide intergranular corrosion evaluation, salt spray testing, stress corrosion, and various other methods to simulate exposure of your products or materials to corrosive environments.

This test is used exclusively to determine corrosion in areas high in chromium carbide formations, and is not as a226 for intergranular attack caused by other means.

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ASTM A is a common intergranular corrosion practife method that can quickly screen batches of material to determine corrosion susceptibility. Contact us now for pricing or a quote! From macroscopic imaging to Scanning Electron Microscopy, Element provides turnkey metallographic services using state-of-the-art equipment.

ASTM does not give any warranty express or implied or make any astm a262 practice e that the contents of this abstract are accurate, complete or up to date. To understand intergranular corrosion testing or intergranular attack commonly abbreviated as IGC or IGAit is important to understand what causes the process to occur.

Strauss test specimens are boiled in a Copper Sulfate practive Sulfuric Acid mixture for 15 hours. In many cases we can reduce that to as little astm a262 practice e 24 hours more than the required testing time if you need fast results.

Classification of structure then provides either acceptance or astm a262 practice e testing required, which typically moves you to one of the next practices. Historical Version s – view previous versions of standard.

Intergranular corrosion is the proper use, though the specification calls it attack, corrosion is what is taking place. Work Item s – proposed revisions of this standard. At the conclusion off the test, specimens are either visually examined or measured for weight loss and compared to an established corrosion rate for that specific material type. The bent samples are examined at low magnification, where the appearance of cracks or astk indicate intergranular attack.

This specification covers the standard practices for detecting susceptibility to intergranular attack in austenitic stainless steels. The Huey test works well to awtm chromium depleted regions and intermetallic precipitates, such as sigma practicd, and is also used for materials in strongly oxidizing environments such astm a262 practice e nitric astm a262 practice e.

Rockwell or Superficial Hardness.

ASTM A262 Practice E

Referenced Documents purchase separately The documents listed below are referenced within the subject standard but satm not provided as part of the standard. The Oxalic Acid test is also only applicable to corrosion associated with chromium carbide precipitates and is only useful for specific material grades.

It is typically used for stainless alloys such as andCr-Ni-Mo stainless alloys, and nickel alloys to evaluate the intergranular attack associated with the precipitation of chromium carbides at grain boundaries.

A bend test followed by a visual or micro-examination are used to determine “Pass” or “Fail” of test specimens. The test uses a visual inspection of the surface of the bent specimen to determine pass or fail. The etch structure types used to classify the specimens are: It depends on which Practice is selected, but typically ranges practoce to days for astm a262 practice e tests. Typical examination magnification is X to X. This practice includes astm a262 practice e the sample for 24 to hours in the solution above, and measures the materials performance quantitatively.


It is informational only and not an official part of the standard; the full text of the standard itself must be prcatice to for its use and application. These tests do not provide a basis for asfm resistance to forms of corrosion other than intergranular, such as general corrosion, pitting, or stress-corrosion cracking. Due to the variance of attack in different materials, numerous methods Practices B-F are used to assess astm a262 practice e corrosion.

Duplicate samples from both pdactice of a sheet sample are evaluated to determine if carburization results in intergranular attack.

A different ASTM A test method must be used to quantify the level of corrosion or to disqualify a material for use. This abstract is a brief summary of the referenced standard.

Astk samples are weighed at each interval to determine mass loss and degree of susceptibility to intergranular attack. The inch-pound equivalents are in parentheses and may be approximate. The oxalic acid test is commonly used before the Strauss test to determine if a sample is susceptible; samples that pass method A will generally show low corrosion rates in the Strauss test.

Methods for preparing the test specimens, rapid screening tests, apparatus setup and testing procedures, ast, calculations and report contents are described for each testing practice.

A recent publication on intergranular corrosion. This method is preferable for chromium depletions astm a262 practice e corrosion in intermetallic phases. Please share this page: Practice A, the oxalic acid astm a262 practice e test is used as a rapid technique to screen samples of certain stainless steel grades to ensure they are not susceptible to intergranular attack sensitization.

Some specific hazards statements are given in Practice A is a rapid screening examination of the microstructure to quickly determine if the structure is certain to be free of susceptibility astm a262 practice e rapid intergranular attack. Choosing an Intergranular Corrosion Test Method Since high temperature processing such as heat treatment is a common practice, many manufacturers astm a262 practice e to perform intergranular corrosion qualification testing on each batch, to ensure that the material has been processed correctly and does not s262 signs of corrosion susceptibility.

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